
First, the fibers are pretreated. Basalt fibers are cut into short fibers of 10cm length, soaked in anhydrous ethanol for 30min to remove surface oil, and then dried in an 80℃ oven for 2h for later use. KH-560 ethanol solutions (1%, 3%, 5%, 7%) are prepared according to the set concentration, stirred evenly, and poured into a three-necked flask, followed by ultrasonic dispersion for 10min to ensure uniform dispersion of the coupling agent. After completing the above preparation, the dried basalt fibers are placed in the flask and reacted at a set temperature (40℃, 60℃, 80℃) with a stirring speed of 100r/min for a certain time (1h, 2h, 3h). After the reaction, the fibers are taken out, washed 3 times with anhydrous ethanol to remove unreacted coupling agent, and then dried in a 100℃ oven for 3h to obtain modified basalt fibers, which are sealed and stored for later use. First, the resin matrix is prepared. Epoxy resin E-51, curing agent MTHPA, and accelerator EMI-2,4 are weighed according to the formula ratio, and stirred and mixed in a 60℃ oil bath for 30min to obtain a uniform resin matrix. Then, the modified basalt fibers are added to the resin matrix according to the set content (10wt%, 15wt%, 20wt%, 25wt%), mechanically stirred (speed 300r/min) for 20min, and then ultrasonically dispersed for 15min to ensure that the fibers are evenly dispersed in the resin matrix and avoid agglomeration. Then, the mixed material is poured into a mold (150mm×100mm×4mm) pre-coated with a release agent, placed in a hot press, and cured at a pressure of 5MPa according to the set curing temperature (60℃, 70℃, 80℃, 90℃) and curing time (2h, 3h, 4h, 5h). After curing, it is naturally cooled to room temperature, demolded to obtain BF/EP composite material samples, which are processed into tensile, impact, and bending samples according to the test standards, and burrs and defects on the sample surface are removed.
2.3.1 Control of Roasting Temperature and Time The roasting...